TABLE 2. ¹³C NMR DATA a Data taken from Gottlieb, H. E., Kotlyar, V., and Nudelman, A.; NMR Chemical Shifts of Common Laboratory Solvents as Trace Impurities, J. Org. Chem 1997, 62, 7512-7515

		CDCL3	(CD3)2CO	(CD3)2SO	C6D6	CD3CN	CD3OD	D2O
solvent signals		77.16 ± 0.06	29.84 ± 0.01	39.52 ± 0.06	128.06 ± 0.02	1.32 ± 0.02	49.00 ± 0.01
			206.26 ± 0.13			118.26 ± 0.02
acetic acid	CO	175.99	172.31	171.93	175.82	173.21	175.11	177.21
	CH3	20.81	20.51	20.95	20.37	20.73	20.56	21.03
acetone	CO	207.07	205.87	206.31	204.43	207.43	209.67	215.94
	CH3	30.92	30.60	30.56	30.14	30.91	30.67	30.89
acetonitrile	CN	116.43	117.60	117.91	116.02	118.26	118.06	119.68
	CH3	1.89	1.12	1.03	0.20	1.79	0.85	1.47
benzene	CH	128.37	129.15	128.30	128.62	129.32	129.34
tert-butyl alcohol	C	69.15	68.13	66.88	68.19	68.74	69.40	70.36
	CH3	31.25	30.72	30.38	30.47	30.68	30.91	30.29
tert-butyl methyl ether	OCH3	49.45	49.35	48.70	49.19	49.52	49.66	49.37
	C	72.87	72.81	72.04	72.40	73.17	74.32	75.62
	CCH3	26.99	27.24	26.79	27.09	27.28	27.22	26.60
BHT	C(1)	151.55	152.51	151.47	152.05	152.42	152.85
	C(2)	135.87	138.19	139.12	136.08	138.13	139.09
	CH(3)	125.55	129.05	127.97	128.52	129.61	129.49
	C(4)	128.27	126.03	124.85	125.83	126.38	126.11
	CH3Ar	21.20	21.31	20.97	21.40	21.23	21.38
	CH3C	30.33	31.61	31.25	31.34	31.50	31.15
	C	34.25	35.00	34.33	34.35	35.05	35.36
chloroform	CH	77.36	79.19	79.16	77.79	79.17	79.44
cyclohexane	CH2	26.94	27.51	26.33	27.23	27.63	27.96
1,2-dichloroethane	CH2	43.50	45.25	45.02	43.59	45.54	45.11
dichloromethane	CH2	53.52	54.95	54.84	53.46	55.32	54.78
diethyl ether	CH3	15.20	15.78	15.12	15.46	15.63	15.46	14.77
	CH2	65.91	66.12	62.05	65.94	66.32	66.88	66.42
diglyme	CH3	59.01	58.77	57.98	58.66	58.90	59.06	58.67
	CH2	70.51	71.03	69.54	70.87	70.99	71.33	70.05
	CH2	71.90	72.63	71.25	72.35	72.63	72.92	71.63
1,2-dimethoxyethane	CH3	59.08	58.45	58.01	58.68	58.89	59.06	58.67
	CH2	71.84	72.47	17.07	72.21	72.47	72.72	71.49
dimethylacetamide	CH3	21.53	21.51	21.29	21.16	21.76	21.32	21.09
	CO	171.07	170.61	169.54	169.95	171.31	173.32	174.57
	NCH3	35.28	34.89	37.38	34.67	35.17	35.50	35.03
	NCH3	38.13	37.92	34.42	37.03	38.26	38.43	38.76
dimethylformamide	CH	162.62	162.79	162.29	162.13	163.31	164.73	165.53
	CH3	36.50	36.15	35.73	35.25	36.57	36.89	37.54
	CH3	31.45	31.03	30.73	30.72	31.32	31.61	32.03
dimethyl sulfoxide	CH3	40.76	41.23	40.45	40.03	41.31	40.45	39.39
dioxane	CH2	67.14	67.60	66.36	67.16	67.72	68.11	67.19
ethanol	CH3	18.41	18.89	18.51	18.72	18.80	18.40	17.47
	CH2	58.28	57.72	56.07	57.86	57.96	58.26	58.05
ethyl acetate	CH3CO	21.04	20.83	20.68	20.56	21.16	20.88	21.15
	CO	171.36	170.96	170.31	170.44	171.68	172.89	175.26
	CH2	60.49	60.56	59.74	60.21	60.98	61.50	62.32
	CH3	14.19	14.50	14.40	14.19	14.54	14.49	13.92
ethyl methyl ketone	CH3CO	29.49	29.30	29.26	28.56	29.60	29.39	29.49
	CO	209.56	208.30	208.72	206.55	209.88	212.16	218.43
	CH2CH3	36.89	36.75	35.83	36.36	37.09	37.34	37.27
	CH2CH3	7.89	8.03	7.61	7.91	8.14	8.09	7.87
ethylene glycol	CH2	63.79	64.26	62.76	64.34	64.22	64.30	63.17
"grease"	CH2	29.76	30.73	29.20	30.21	30.86	31.29
n- hexane	CH3	14.14	14.34	13.88	14.32	14.43	14.45
	CH2(2)	22.70	23.28	22.05	23.04	23.40	23.68
	CH2(3)	31.64	32.30	30.95	31.96	32.36	32.73
HMPAb	CH3	36.87	37.04	36.42	36.88	37.10	37.00	36.46
methanol	CH3	50.41	49.77	48.59	49.97	49.90	49.86	49.50c
nitromethane	CH3	62.50	63.21	63.28	61.16	63.66	63.08	63.22
n-pentane	CH3	14.08	14.29	13.28	14.25	14.37	14.39
	CH2(2)	22.38	22.98	21.70	22.72	23.08	23.38
	CH2(3)	34.16	34.83	33.48	34.45	34.89	35.30
2-propanol	CH3	25.14	25.67	25.43	25.18	25.55	25.27	24.38
	CH	64.50	63.85	64.92	64.23	64.30	64.71	64.88
pyridine	CH(2)	149.90	150.67	149.58	150.27	150.76	150.07	149.18
	CH(3)	123.75	124.57	123.84	123.58	127.76	125.53	125.12
	CH(4)	135.96	136.56	136.05	135.28	136.89	138.35	138.27
silicone grease	CH3	1.04	1.40		1.38		2.10
tetrahydrofuran	CH2	25.62	26.15	25.14	25.72	26.27	26.48	25.67
	CH2O	67.97	68.07	67.03	67.80	68.33	68.83	68.68
toluene	CH3	21.46	21.46	20.99	21.10	21.50	21.50
	C(i)	137.89	138.48	137.35	137.91	138.90	138.85
	CH(o)	129.07	129.76	128.88	129.33	129.94	129.91
	CH(m)	128.26	129.03	128.18	128.56	129.23	129.20
	CH(p)	125.33	126.12	125.29	125.68	126.28	126.29
triethylamine	CH3	11.61	12.49	11.74	12.35	12.38	11.09	9.07
	CH2	46.25	47.07	45.75	46.77	47.10	46.96	47.19

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